Questions and Answers
Question; Is making my own spirits safe and legal?
Answer; Our process involves the controlled manufacture of alcohol from a
known mix of nutrient sugar and yeast. The distillate is then cleaned with
activated carbon to remove unwanted flavours. Following the procedures will
result in pure clean alcohol that in most cases has less byproducts than alcohol
produced from more traditional sources. Home distilling is legal in some
countries and not in others. In most situations local authorities appear
reluctant to move against citizens producing alcohol for their own use. However
in all countries throughout the world, authorities take a very dim view of
anyone producing alcohol for sale.
Question; How long does it take to make each batch of spirits?
Answer; Depending on the type of yeast and nutrients as well as the type
of carbon process used you can be drinking your own home made spirits within 7
days.
Question; Which type of still produces the most alcohol? Reflux or Pot
Stills.
Answer; All stills collect alcohol from your wash at varying strengths.
The total amount of alcohol collected is dependent on how much is present in
your wash. Reflux Stills collect less in volume but this is much higher in
alcohol strength. Alcohol should always be watered down to below 50%/V before
filtering. After filtering, and watering down, the total amount of finished
alcohol should be the same no matter which still you have used.
Question; If I add more sugar to my wash will I get more alcohol?
Answer; You may do, but do not add more than the recipe or manufacturer
recommends as yeast varieties are selected for different properties. A yeast
variety which can ferment rapidly may not be very resistant to alcohol. If this
is the case, adding too much sugar may result in unfermented sugar remaining in
the wash. This may cause the wash to froth during distilling. Most spirit
yeasts/nutrients have a recipe printed on them. There are three Turbo varieties
available from Still Spirits; Standard Turbo, Turbo Extra and Temperature
Tolerant Turbo. Select the yeast which best suits your needs.
Question; How can I improve the quality of my finished spirit?
Answer; The following are recommended.
Pot stills collect all the condensate from the boil and condense it. Reflux
stills have a seperate chamber which further purifies the condensate before it
condenses it. This produces an distillate which is more concentrated and
contains less impurities than pot stills and so it follows that they produce
better quality spirit.
The degree of carbon treatment and type of carbon. Always use a reputable brand
of carbon that has been designed specifically for the job. Any old carbon or
charcoal will not do. Some distillers actually run the spirit through the filter
twice or three times to improve its smoothness.
The type of wash used. It is essential to use a high quality yeast and nutrient
to produce the wash and to maintain the correct fermentation temperatures.
Distilling unwanted or excess beer, wine or other ingredients may cause
equipment damage or failure as well as producing less than desirable or even
poisonous byproducts.
Aging. By storing some of the spirit you produce in glass in a cool dark place
for a long period of time it will mellow. Some distillers age their spirit in
oak barrels to imitate the commercial brands. This process may be imitated by
the addition of oak chips or essences to the spirit. Age spirit in bulk for best
results.
The percentage at which the alcohol is consumed. For best results do not drink
the spirit at greater than 40% alcohol by volume.
Question; Why can't I make my own wash recipe and my own yeast nutrient
and or culture?
Answer; You may do this but it is your own responsibility and it may cost
rather than save money in the end. All our brands of spirit yeasts, and/or
nutrients and Turbo yeasts have been specifically designed for the job. They
produce very low levels of byproducts and are safe and reliable.
Question; Will I make methanol when I distill?
Answer; You may produce extremely small quantites of methanol when
distilling Still Spirits Turbo products. These will be removed in the first
portion of distillate which is seperated and called the head. As we are only
fermenting sugar with a known yeast and nutrient mix, the byproducts such as
methanol are minimal. If you wish to distill other mixtures then methanol could
be produced and could prove disasterous.
Question;Why don't I have to age my spirit like commercial distilleries?
Answer; Over the ages distilleries have been positioned as a result of
excess raw materials. The excess raw materials have usually been inexpensive or
in some cases like Rum have been a waste product and costly to dispose off.
These cheap raw materials have been converted into potable alcohol and aged to
improve their smoothness, sometimes in oak barrels to also remove unwanted
flavours and any unwanted alcohols. Raw spirit from some of these products can
be undrinkable and even dangerous so ageing is necessary for many reasons.
Making alcohol using pure sugar, Turbo Yeast, Still Spirit Carbons and drinkable
water produces an extremely clean alcohol. We then add essences to the drink to
copy your favourite tipple.
Question; Why does the spirit drip through the continuous filter so
slowly?
Answer; This may be caused by the following.
Too much high activity carbon has passed down the tube to the black cartridge
after the tap has been turned on. Helpful Hint: Put a 25 mm spacer under the
continuous filter, at the front where the hose exits to the continuous filter.
This will tilt the container back, and ensure that the High Activity Carbon
settles to the back of the filter. This will avoid any carbon from settling over
the outlet to the filter cartridge which could block it.
It is important to let most of the High Activity Carbon settle before opening
the tap and letting the spirit flow through to the filter cartridge. This takes
24 hours. If you open the valve too soon then too much carbon may flow down the
tube and clog the filter paper making the process go much slower.
The Filter Cartridge may have been overfilled with Finishing Carbon. As the
carbon reacts with the spirit it expands and heats up. Always leave a 10 mm gap
for expansion.
Temperature: The filter system operates best at normal room temperature. As the
spirit cools down it becomes thicker. As a result, in winter the whole process
slows down. Try heating your spirit before adding it to the reservior or putting
the Continuous Filter in a warm place.
Too many filter papers or the wrong type of filter paper.
A dirty or clogged tube, tap or cartridge. The whole Continuous Filter should be
rinsed thoroughly after every use.
Impatience: Remember that the Continuous Filter is removing unwanted impurities
from your spirit. Trying to speed things up too much will effect the quality of
your spirit.
Question; Why does the spirit drip through the Continuous Filter too fast?
Answer; If the spirit runs through too quickly it is usually due to the filter
paper not sitting correctly. This can occur when the continuous filter has not
been cleaned properly after use. Always ensure all Finishing Carbon is cleaned
out of the cartridge. The filter paper can also be dislodged by the spirit
reacting with the Finishing Carbon. Simply repack the cartridge using the same
carbon and paper. Helpful Hint: The carbons are designed to work in tandem. When
you open the tap and start the flow of spirit to the filter cartridge, some of
the HA Carbon comes down with the spirit. This forms a coating on the filter
paper which then filters out any more carbon. If you reset the filter and don't
have sufficient HA Carbon on the paper then the filter paper may not work
correctly. To remedy this simply ensure some of the HA Carbon is mixed into the
first lot of spirit that comes down the tube. Also ensure that you use Still
Spirits HA Carbon as your first treatment in the Continuous Filter.
Question; Why does my filtered spirit have a grey tint or sediment after
filtering.
Answer; Some traces of carbon have come through the filter. Run your
spirit through the finishing carbon again making sure the filter paper is
properly positioned.
Question; Why is my spirit coming out of the still cloudy?
Answer; The wash has not been allowed to settle with excess sediment
dropping to the bottom of the fermenter.
Fermentation temperature is too high causing the production of unwanted but
harmless proteins.
The distilling equipment is dirty or faulty.
The wash is not fully fermented.
Question; What measures can I take to guard against cloudy spirit?
Answer; The best method is to add some "distilling conditioner" to your
wash in the still boiler before starting. This stops the excessive foaming in
the boiler which is caused by high concentrations of proteins and unfermented
sugars. Distilling conditioner allows distillation even if your wash has not
fully fermented out.
Question; What can I do to make the cloudy spirit drinkable.
Answer; The usual carbon filtering process will in most cases remove the
cloudiness, but a sure way is to redistill the cloudy spirit mixed with water,
or, with your next wash. Helpful Hint: Make sure that you add enough water to
ensure that the element will still be covered when all the alcohol has been
boiled off.
Question; Why is my yield of distilled spirit so low?
Answer; Your wash has most probably not fermented out properly. Always
check your wash with a beer, wine and wash hydrometer before distilling. Check
your still for any steam leaks. Make sure you are following the operating
instructions.
Question; Why does my Thermoplastic still run for about 2 hours then
cutout?
Answer; These early model stills have a boil dry protect element
installed to guard against improper use. The element must be installed with the
flat pin to the top. If the element is fitted incorrectly then the boil dry
protect will cut in early. If your element is fitted correctly and the problem
persists then see your retailer. It may be that you need to replace your
element.
Sediment forming in spirit after carbon filtration.
A fine sediment which develops in the spirit some time after carbon treatment.
This is a very rare occurrence. The fine sediment is in fact mineral salts which
originate within the activated carbon itself. When spirit runs over activated
carbon which contains some mineral salts, some mineral salts can be absorbed
into the spirit. Later, once the temperature has dropped, these mineral salts
start to become insoluble in the spirit and after a few days a fine sediment
appears in the spirit. This fine sediment (sometimes looks like a milky haze,
other times it drops to the bottom of the bottle) is the mineral salts
originally from the activated carbon. These mineral salts are absolutely 100%
safe (in fact essential for life!) but you don't want them in your spirit.
Under certain circumstances, some of this residual mineral content gets
dissolved into distillate spirit as the spirit flows over the activated carbon.
Think of it this way, as the spirit passes through the activated carbon, the
carbon absorbs the vast majority of 'volatiles' from the spirit and holds them
within the internal pore structure - however, under certain circumstances,
mineral salts contained within the carbon may pass into the spirit. Whether
mineral salts do indeed get dissolved into the spirit depends upon 2 main
variables:
1. The amount and types of mineral salts within the particular batch of carbon.
2. The pH and chelate chemical (eg organic acids like citrate are a chelating
agent) content of the spirit.
Obviously, we have no control over 1. In a perfect world we would persuade the
supplier to first wash with an inorganic acid like they currently do and then
wash with organic acids to remove the remaining salt content.
Regarding point 2, Turbo extra wash contains particularly high level of chelates
and a particularly low (acidic) pH. In fact, of all 54 different Turbo recipes
we manufacture, Turbo Extra has the highest level of all Turbos mainly because
it is based on a Urea-free recipe and uses a high alcohol yeast strain which
tends to produce more volatiles in the wash than a standard Turbo would.
So what? you may be saying - but this is where things start to come together!
The 2% remaining mineral salts in the activated carbon are partially soluble in
Turbo Extra distillate. Especially where the distillation performance has been
poor and not removed many of the volatiles from the wash (leaving more organic
acids in the spirit).
So as the spirit passes through the Carbon, it dissolves some of these 2%
mineral salts. These mineral salts remain soluble in the spirit for some minutes
or hours because the spirit temperature is warm and so has higher solubility.
After the spirit has cooled, these mineral salts will begin to become insoluble.
If you had a spectrophotometer to measure even the slightest haze, you would
begin to 'see' the spirit 'go hazy' after just a few hours. To the naked eye,
you will not start to see these solids until after 2 or 3 days (may be less or
more depending upon the level of mineral salts present).
Re-filtering through activated carbon will not help, but 're-filtering' through
an ordinary wine filter or even a coffee filter, say 1 week after the filtering
through carbon would remove the insoluble mineral salts and hence solve the
problem. But spirit should be stored cold (not frozen) during this week to
ensure anything that is going to become insoluble, does become insoluble). If
the spirit is left for long enough (3 or 4 weeks?), it should be easy to pour
off the bright spirit from a white sediment at the bottom of the bottle.
This problem is likely to be more common with Turbo Extra. It is also likely to
be influenced by certain environmental conditions like temperature and water
quality. If the problem persists then it may be worth considering one of our
other Turbo products.
Summary
The sediment is in fact mineral salts and as such are completely harmless. The
sediment forming is caused by a combination of - the fact that mineral salts are
present in small quantities in the carbon we use and the acid levels and pH of
the alcohol being treated.
First Recommendations:- Always use Still Spirit brand Carbons.
Ensure that the temperature is kept as close as possible to 20 degrees C during
fermentation of wash.
Filter spirit containing sediment with a wine filter or coffee filter paper..
Leave until sediment has all dropped out (cold temperatures will accelerate
process) and decant off sediment.
Recommendations if problem persists:- Switch from Turbo Extra to Still Spirits
Turbo or Temperature Tolerant Turbo.
Use a reflux still.
My Reflux condenser does not appear to work.
There are two condensing areas in a Reflux Still. The steam first passes through
the Reflux condenser then into the main condenser.
If the condenser is not performing then check the following;
Fill the condenser with water then pull the hoses off the base of the main
condenser. One of these will be the inlet for the water and the other will be
the hose that transfers the water into the reflux condenser. The water should
flow out of the condenser through the pipe that the inlet water pipe is
connected to. If it flows out of the other one then the hoses are either on the
wrong way around or the internal overflow outlet is missing or loose.
Take the marble out of the Reflux condenser and shake the whole condenser. There
should not be any rattling. If there is then the overflow pipe may be loose.
There should be a marble in the Reflux condenser. This should be resting on four
indentations in the inside of the Reflux chamber. The marble ensures that all
the alcohol laden steam comes in contact with the inside of the Reflux chamber.
It has happened that the marble is too small and drops right through the Reflux
chamber and come to rest over the nut at the bottom of the condenser where it
screws onto the still domed top. This cuts off the flow of steam into the
condenser altogether stopping it from working. If the marble is missing, then
the condenser works more like a Pot Still condenser.
Blockages can occur in the condenser. When the condenser is removed from the
still, it should be easy to blow in through the spirit outlet tube. Any
resistance here would indicate a blockage that will most likely be at the back
of the nipple that the outlet tube is attached too. Using a 4 mm flat punch and
a hammer just tap the punch up the outlet to push the inside wall of the main
condenser away from the back end of the nipple. This should clear any blockage.
Water flow is extremely important for the correct operation of the condenser.
First the water runs through the main condenser then into the reflux condenser.
The water warms up in the main condenser as it removes heat from the condensing
spirit. This hot water is then fed into the reflux condenser. If the flow of
water is too high then the reflux condenser becomes too efficient which reduces
the flow of steam into the main condenser. This reduced flow will also result in
a higher alcohol content as more of the heavier molecules like water are
returned to the Still and what does get past the reflux condenser is the lighter
molecules or the alcohol.
When a condenser is running properly, the top two bands of the main condenser
should be very hot. The bottom band of the spiral should be cool and the one
above it should be hot but not be too hot to touch.
The water flow required with a Reflux Still is very low. Typically 400 mls per
minute. This is required because the condenser is very efficient. In warmer
climates where the cold water is above 20o C. it may be necessary to fit a
cooling coil to the water inlet tube and to immerse this in a tank with ice
added to bring the temperature of the incoming water down. The low water flow is
a big advantage in area\’s where water is scarce or where water meters add cost
to the process.
My Pot Still Condensor does not appear to be working properly
Not a lot can go wrong with this condenser other than the hoses being put on the
wrong way around. It is important to have the water flow in from the bottom and
the over flow to come out from the top. That way the condenser jacket fills with
water. If the hoses are on the wrong way around then the water will take the
quickest route and will not fill the entire jacket. This will reduce the
efficiency of the cooling and could result in some alcohol lost in steam from
the still.
Water flow.
The water flow required with a Pot Still is very high. Typically 2 – 3 litres
per minute. This is required because the condenser is not very efficient. In
warmer climates where the cold water is above 20o C. it may be necessary to fit
a cooling coil to the water inlet tube and to immerse this in a tank with ice
added to bring the temperature of the incoming water down.
My thermometer seems to give strange readings.
Make sure that the thermometer is inserted into the bung so that the red bulb of
alcohol at the bottom of the thermometer is positioned at the point where the
steam is coming up and changes direction to go into the main condensing chamber.
If the thermometer goes in too far then a higher reading will result. If it is
not in far enough a lower reading may result. Don\’t rely 100% on the thermometer
as we are not providing laboratory quality instruments. The temperature is a
guide only. If there are no steam leaks and the correct amount of sugar was
added and fermented, then collecting the right quantity is the safest method of
determining when to stop collecting. If the spirit is then at the desired
strength then you can assume that all is well.
I have discoloured spirit or floaters in my spirit.
New condensers can sometimes produce discoloured spirit the first or second time
that they are used. All condensers are acid washed to remove flux etc. after
manufacture but problems can still arise.
Dark bits in the spirit.
This is more common in the Pot Still than the Reflux but can happen in both. It
is almost always caused by collecting too much spirit. This usually shows up the
next time the still is run to fix this problem clean the condenser as below and
only collect the recommended amount.
Yellow spirit can also be produced if too much spirit has been collected on the
previous run. Byproducts build up inside the condenser and are flushed out with
the next run. The carbon treatment should remove this but redistilling gives the
customer peace of mind. Clean the condenser before use.
How to clean the condenser.
Soak the element in white vinegar or Coca-Cola. Rinse it with a weak solution of
dishwashing liquid and water then wash any residue off after treatment with
plenty of clean water. This treatment should clean the condenser then start the
oxidation process again which hardens the surface of the copper.
I get blue spirit from my still.
Blue spirit can be caused by a reaction from certain washes containing
excwessive amounts of nutrients and the copper in the condenser. As some washes
have an imbalance of nutrients certain by products like ammonia and Acetic acid
in large quantities can form in the wash. This is then distilled and attacks the
copper. This is extremely uncommon when using Still Spirits Turbo products. Do
not add more than one sachet per 2 5litre brew.
My still does not seem to heat up as indicated in the instructions;
We fit two different elements to our stills depending on the size of the Still.
For the 5 litre still in Australia we fit a SS1000 which is rated at 1000 watts
at 230 volts. In Australia the voltage is 240 volts which means the element will
draw about 1040 watts.
For the 25 litre Still and the 3 in 1 Fermenter, we fit a SS1380 element which
is rated at 1380 watts at 230 volts. In Australia this means the element will
draw 1440 watts.
We originally fitted the SS1380 element to all stills but we found the higher
wattage was too violent in the 5 litre stills. We also had a problem with one
batch of 3 in 1 fermenters where SS1000 watt elements were fitted. If these were
run as a still they would take excessive time to heat up and hours to distill
anything. We have also had a couple of instances of elements not performing. A
rough guide is to ascertain how long the element takes to heat the still up from
cold to start distilling. For a 5 litre still it should be 35 minutes. For a 25
litre Still it should be 1 hour 25 minutes.
What do I do if my cold tap water is above 20o C.
When this happens you will need to run more than 400 mls of water per minute
through your Reflux condensor. In your Reflux still instructions it tells you to
run water at 400 mls per minute. This relies on the tap water being below 20o C
and it ensures that your condensor is running efficiently. If you are in a
warmer climate like Australia you may need to increase your water flow but this
creates a problem with the efficiency of the condenser and excessive use of
water. To overcome this problem, purchase 2 metres of copper pipe with the
diameter small enough to fit into the tap line of your Reflux condensor.
Alternately purchase 6 metres of the same plastic hose and fit this onto your
tower. When you have done this all you need to do before you use your still is
fill an old ice cream container or small bucket with water and make your own
ice, place the copper pipe or the plastic hose into a bucket and cover with ice
this will reduce the temperature of the incoming water and you will be able to
reduce your flow back to 400 mls approx. This will also help you get a better
return from your still as it will make your condenser more efficient.
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